Preparation and morphology of palladium oxide fibers via electrospinning

P. Viswanathamurthi; N. Bhattarai; H. Y. Kim; D. I. Cha; D. R. Lee

doi:10.1016/j.matlet.2004.04.035

Preparation and morphology of palladium oxide fibers via electrospinning

P. Viswanathamurthi, N. Bhattarai, H. Y. Kim, D. I. Cha, D. R. Lee

Research output: Contribution to journal › Article › peer-review

Abstract

An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature.

Original language	English
Pages (from-to)	3368-3372
Number of pages	5
Journal	Materials Letters
Volume	58
Issue number	26
DOIs	https://doi.org/10.1016/j.matlet.2004.04.035
State	Published - Oct 2004
Externally published	Yes

Keywords

Calcination
Electrospinning
Pdac/PC fibers

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10.1016/j.matlet.2004.04.035

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title = "Preparation and morphology of palladium oxide fibers via electrospinning",

abstract = "An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature.",

keywords = "Calcination, Electrospinning, Pdac/PC fibers",

author = "P. Viswanathamurthi and N. Bhattarai and Kim, \{H. Y.\} and Cha, \{D. I.\} and Lee, \{D. R.\}",

year = "2004",

month = oct,

doi = "10.1016/j.matlet.2004.04.035",

language = "English",

volume = "58",

pages = "3368--3372",

journal = "Materials Letters",

issn = "0167-577X",

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TY - JOUR

T1 - Preparation and morphology of palladium oxide fibers via electrospinning

AU - Viswanathamurthi, P.

AU - Bhattarai, N.

AU - Kim, H. Y.

AU - Cha, D. I.

AU - Lee, D. R.

PY - 2004/10

Y1 - 2004/10

N2 - An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature.

AB - An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature.

KW - Calcination

KW - Electrospinning

KW - Pdac/PC fibers

UR - https://www.scopus.com/pages/publications/4444229395

U2 - 10.1016/j.matlet.2004.04.035

DO - 10.1016/j.matlet.2004.04.035

M3 - Article

SN - 0167-577X

VL - 58

SP - 3368

EP - 3372

JO - Materials Letters

JF - Materials Letters

IS - 26

ER -

Preparation and morphology of palladium oxide fibers via electrospinning

Abstract

Keywords

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