Preparation and morphology of palladium oxide fibers via electrospinning

P. Viswanathamurthi; Narayan Bhattarai; Hak Yong Kim; Dong Il Cha; Douk Rae Lee

doi:10.1016/j.matlet.2004.04.035

Preparation and morphology of palladium oxide fibers via electrospinning

P. Viswanathamurthi
, Narayan Bhattarai
, Hak Yong Kim
, Dong Il Cha
, Douk Rae Lee

Chemical, Biological, and Bio Engineering

Research output: Contribution to journal › Article › peer-review

34 Scopus citations

Abstract

An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature. © 2004 Elsevier B.V. All rights reserved.

Original language	English
Pages (from-to)	3368-3372
Number of pages	5
Journal	Materials Letters
Volume	58
Issue number	26
DOIs	https://doi.org/10.1016/j.matlet.2004.04.035
State	Published - Jan 1 2004

Keywords

Calcination
Electrospinning
Pdac/PC fibers

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10.1016/j.matlet.2004.04.035

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title = "Preparation and morphology of palladium oxide fibers via electrospinning",

abstract = "An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature. {\textcopyright} 2004 Elsevier B.V. All rights reserved.",

keywords = "Calcination, Electrospinning, Pdac/PC fibers",

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T1 - Preparation and morphology of palladium oxide fibers via electrospinning

AU - Viswanathamurthi, P.

AU - Bhattarai, Narayan

AU - Kim, Hak Yong

AU - Cha, Dong Il

AU - Lee, Douk Rae

PY - 2004/1/1

Y1 - 2004/1/1

N2 - An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature. © 2004 Elsevier B.V. All rights reserved.

AB - An attempt has been successfully made to prepare palladium acetate/polycarbonate (Pdac/PC) composite fibers with diameter in submicron range by electrospinning method using different concentrations of palladium acetate incorporated into polycarbonate solution. Pure ceramic metal oxide fibers were obtained by high temperature calcination of the palladium acetate/polycarbonate composite fibers. On the basis of the infrared spectroscopic data, it has been concluded that the relatively electron rich oxygen atoms of the ketone groups in the polycarbonate molecules are assumed to interact with palladium acetate. It has been observed that the surface morphology and crystallinity of the fibers depend on the calcination temperature. © 2004 Elsevier B.V. All rights reserved.

KW - Calcination

KW - Electrospinning

KW - Pdac/PC fibers

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VL - 58

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JO - Materials Letters

JF - Materials Letters

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Preparation and morphology of palladium oxide fibers via electrospinning

Abstract

Keywords

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